HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178446057, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 178445930 | HCID 178445930 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 178446057 | HCID 178446057 | 100% |
Reaction Steps
160 mg of [(S)-3-Methyl-1-(4H-[1,2,4]triazol-3-ylsulfanylmethyl)-butyl]-carbamic acid tert-butyl ester were reacted with 2.6 ml of 4M hydrochloric acid in dioxane at it for 2 h. The reaction was concentrated in vacuo and the resulting crude product was used without further purification. 125 mg (100%) of (S)-3-methyl-1-(4H-[1,2,4]triazol-3-ylsulfanylmethyl)-butylamine-hydrochloride were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09156796B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-695db5fe1c6f4a55b4f76c28da6fec22 |
| Source note | uspto-grants-2015_10 |