反应详情

160 mg of [(S)-3-Methyl-1-(4H-[1,2,4]triazol-3-ylsulfanylmethyl)-butyl]-carbamic acid tert-butyl ester were reacted with 2.6 ml of 4M hydrochloric acid in dioxane at it for 2 h. The reaction was concentrated in vacuo and the resulting crude product was used without further purification. 125 mg (100%) of (S)-3-methyl-1-(4H-[1,2,4]triazol-3-ylsulfanylmethyl)-butylamine-hydrochloride were obtained.

1. concentrationThe reaction was concentrated in vacuo
2. customthe resulting crude product was used without further purification