HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloro-5-iodo-2-methyl-7H-pyrrolo(2,3-d)pyrimidine → HCID 86706959, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloro-5-iodo-2-methyl-7H-pyrrolo(2,3-d)pyrimidine | HCID 66570709 | — |
| Reactant | 4-chloro-5-iodo-7-((2-(trimethylsilyl)ethoxy)methyl)-7H-pyrrolo[2,3-d]pyrimidine | HCID 86706933 | — |
| Product | HCID 86706959 | HCID 86706959 | — |
Reaction Steps
4-Chloro-5-iodo-2-methyl-7H-pyrrolo[2,3-d]pyrimidine (C22) was converted to the product according to the method used for synthesis of 4-chloro-5-iodo-7-{[2-(trimethylsilyl)ethoxy]methyl}-7H-pyrrolo[2,3-d]pyrimidine (C1) in Preparation P1. The product was obtained as a yellow oil. Yield: 400 mg, 0.94 mmol, 84%. LCMS m/z 424.0[M+H+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09156845B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-d060b66585354704a103925a9dcc7ce5 |
| Source note | uspto-grants-2015_10 |