反应详情

In a 500 mL hydrogenation container was added N-(1,3-di(prop-1-en-2-yl)dibenzo[b,d]furan-4-yl)acetamide (22.6 g, 74.0 mmol), Pd/C, 10% (3 g, 74.0 mmol) and Pt/C, 5% (3 g, 74.0 mmol) in Ethanol (200 mL). After two days reaction, the solution was filtered through a Celite plug and washed with dichloromethane. The filtration was concentrated to give crude N-(1,3-diisopropyldibenzo[b,d]furan-4-yl)acetamide (18.8 g, 82% yield) as white solid.

1. customAfter two days reaction
2. filtrationthe solution was filtered through a Celite plug
3. washwashed with dichloromethane
4. filtrationThe filtration
5. concentrationwas concentrated