Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1751313Generated: October 27, 2026

2-Morpholinoethanol → HCID 86612011, compound

https://huagongshe.com/reaction/1751313

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-MorpholinoethanolHCID 61163—
Reactant2-(2,2,3,3,4,4,5,5,5-Nonafluoropentyl)oxiraneHCID 2775819—
ProductHCID 86612011HCID 8661201173%

Reaction Conditions

Temperature80 °C

Reaction Steps

A mixture of 13.1 g of 2-morpholinoethanol and 27.6 g of 1,2-epoxy-4,4,5,5,6,6,7,7,7-nonafluoroheptane was stirred at 80° C. for 10 hours. The reaction mixture was directly purified by silica gel column chromatography. There was obtained 29.7 g of 1-(2-morpholinoethoxy)-4,4,5,5,6,6,7,7,7-nonafluoro-2-heptanol (yield 73%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09158191B2
Source datasetuspto-grants-2015_10
ORD IDord-0c13854b48a64d7192714c93eaee8b3f
Source noteuspto-grants-2015_10