1,2-Dichloroethane → HCID 129638279, compound

Participants

Reaction Conditions

Reaction Steps

A solution was prepared by putting 10.0 g (0.0495 mol) of pyrene, 13.9 g (0.0989 mol) of benzoyl chloride, and 87 g of 1,2-dichloroethane in a flask. Subsequently, 13.2 g (0.0989 mol) of aluminum chloride was slowly added to the solution at room temperature and then, heated up to 60° C. and agitated for 8 hours. When the reaction was complete, a precipitate was obtained by adding methanol to the resultant and filtered, obtaining dibenzoylpyrene.

Provenance & Evidence