HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → 2-Acetoxy-2-(3-bromophenyl)acetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | 2-(3-Bromophenyl)-2-hydroxyacetic acid | HCID 2757028 | — |
| Product | 2-Acetoxy-2-(3-bromophenyl)acetic acid | HCID 71212158 | — |
Reaction Steps
Acetyl Chloride (1.5 mL) was added to 3-bromomandelic acid 1 (1.00 g, 4.33 mmol) and stirred at room temperature for 1 hour. The reaction mixture was concentrated in vacuo to provide compound 2 which was used in the next reaction without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09161924B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-012dce4163504b78a7ad063b78e6b549 |
| Source note | uspto-grants-2015_10 |