HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → n-Methyl-3-nitropyridin-4-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | 4-Methoxy-3-nitropyridine | HCID 355832 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | n-Methyl-3-nitropyridin-4-amine | HCID 556016 | — |
Reaction Steps
2.36 g 4-methoxy-3-nitro-pyridine and 2.33 ml methylamine (40% in water) are refluxed in 25 ml of ethanol for 3 h. Then the reaction mixture is evaporated to dryness. 2.3 g product are obtained in the form of a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09161927B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-026394b9529e4ab6851935addf9df61c |
| Source note | uspto-grants-2015_10 |