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HRID1751808

反应详情

EQUATION

反应方程式

HRID 1751808 的结构方程式

REACTANTS

反应物

2
反应SMILES：NC(c1ccccc1)C(O)c1ccccc1
HCID22243

β-amino-α-phenyl-Benzeneethanol

C14H15NO

反应SMILES：CC(C)(C)OC(=O)N1CCC(C(=O)[O-])CC1
HCID6921829

未命名化合物

PRODUCTS

产物

1
反应SMILES：CC(C)(C)OC(=O)N1CCC(c2nc(-c3ccccc3)c(-c3ccccc3)o2)CC1
HCID58080370

未命名化合物

PROCEDURE

实验过程

Starting from 1.08 g of mono-tert-butyl piperidine-1,4-dicarboxylate and 1 g 2-amino-1,2-diphenyl-ethanol the product may be prepared as described in the literature (cf. Tet. 2001, 4867). The product is purified by chromatography (method B). 560 mg are obtained in the form of an oil. Analytical HPLC-MS (method A): RT=1.72 min.

WORKUP

后处理

  1. custommay be prepared
  2. customThe product is purified by chromatography (method B)
  3. custom560 mg are obtained in the form of an oil