HuagongsheHuagongshe Chemistry Print Report · For research reference only
β-amino-α-phenyl-Benzeneethanol → HCID 58080370, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | β-amino-α-phenyl-Benzeneethanol | HCID 22243 | — |
| Reactant | HCID 6921829 | HCID 6921829 | — |
| Product | HCID 58080370 | HCID 58080370 | — |
Reaction Steps
Starting from 1.08 g of mono-tert-butyl piperidine-1,4-dicarboxylate and 1 g 2-amino-1,2-diphenyl-ethanol the product may be prepared as described in the literature (cf. Tet. 2001, 4867). The product is purified by chromatography (method B). 560 mg are obtained in the form of an oil. Analytical HPLC-MS (method A): RT=1.72 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09161927B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-4d5a96054dfc41b4ab538d5659f3bea7 |
| Source note | uspto-grants-2015_10 |