HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylacetylene → Diphenylacetylene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylacetylene | HCID 10821 | — |
| Reactant | Iodobenzene | HCID 11575 | — |
| Product | Diphenylacetylene | HCID 10390 | 95% |
Reaction Steps
Following General Procedure A (120° C., 30 hours), phenyl acetylene (84 μL, 1.5 mmol) is coupled with iodo-benzene (112 μL, 1.0 mmol) to give 95% yield 1,1′-ethyne-1,2-diyldibenzene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09162953B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-9e5663fc60d04a2eb28c6aaf98997709 |
| Source note | uspto-grants-2015_10 |