Hydrogen iodide → HCID 51355285, compound

HRID 1751987Notes

Reaction equation

HRID 1751987 reaction equation
[C:1]([O:5][CH2:6][C:7]1[CH:12]=[CH:11][C:10](B(O)O)=[CH:9][CH:8]=1)([CH3:4])([CH3:3])[CH3:2].Cl[C:17]1[CH:22]=[C:21](Cl)[N:20]=[CH:19][N:18]=1.[IH:24]>>[I:24][C:17]1[CH:22]=[C:21]([C:10]2[CH:11]=[CH:12][C:7]([CH2:6][O:5][C:1]([CH3:4])([CH3:3])[CH3:2])=[CH:8][CH:9]=2)[N:20]=[CH:19][N:18]=1

Participants

4

Reactant 3

HCID 24841Hydrogen iodideHCID 709434,6-DichloropyrimidineHCID 37084804-tert-Butoxymethylphenylboronic acid

Product 1

HCID 51355285HCID 51355285, compound

Procedure

The compound was prepared according to Example 1 using 4-tert-butyloxymethylphenylboronic acid and 4,6-dichloropyrimidine. The resultant chloro compound was converted to iodo with hydroiodic acid as described in the general procedure.

Workup

  1. customThe compound was prepared

Sources & evidence

ORD record
ord-9c6fc447bed143d29cffb005d1ecebe5
Source dataset
uspto-grants-2015_10
Patent number
US09162987B2

Reaction notes

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