Hydrogen iodide → HCID 51354999, compound

HRID 1752006Notes

Reaction equation

HRID 1752006 reaction equation
N[NH:2][C:3]([C:5]1[CH:6]=[C:7](B(O)O)[CH:8]=[CH:9][CH:10]=1)=[O:4].Cl[C:15]1[CH:20]=[C:19](Cl)[N:18]=[CH:17][N:16]=1.[IH:22]>>[I:22][C:15]1[CH:20]=[C:19]([C:7]2[CH:8]=[CH:9][CH:10]=[C:5]([C:3]([NH2:2])=[O:4])[CH:6]=2)[N:18]=[CH:17][N:16]=1

Participants

4

Reactant 3

HCID 24841Hydrogen iodideHCID 709434,6-DichloropyrimidineHCID 44119369[3-(Hydrazinecarbonyl)phenyl]boronic acid

Product 1

HCID 51354999HCID 51354999, compound

Procedure

The compound was prepared according to Example 1 using 3-aminocarbamoylphenylboronic acid and 4,6-dichloropyrimidine. The resultant chloro compound was converted to iodo with hydroiodic acid as described in the general procedure.

Workup

  1. customThe compound was prepared

Sources & evidence

ORD record
ord-28558c1e687e4428bd878eb5ad9fe52e
Source dataset
uspto-grants-2015_10
Patent number
US09162987B2

Reaction notes

Loading…