HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Iodophenol → 2-(4-Iodophenoxy)-4,6-dimethoxypyrimidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Iodophenol | HCID 10894 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 2-Chloro-4,6-dimethoxypyrimidine | HCID 5152323 | — |
| Product | 2-(4-Iodophenoxy)-4,6-dimethoxypyrimidine | HCID 57762623 | 88.7% |
Reaction Steps
In the same manner as in Reference Example 8, 4-iodophenol (223 mg) and 2-chloro-4,6-dimethoxypyrimidine (192 mg) were reacted by using sodium hydride to obtain 2-(4-iodophenoxy)-4,6-dimethoxypyrimidine (322 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09162988B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-f9b45b4b747142e9a4c0f34b1914ca0d |
| Source note | uspto-grants-2015_10 |