HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 57762546, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 2-Butene, 1-bromo-3-methyl- | HCID 70092 | — |
| Reactant | N-(4-iodophenyl)pyrimidin-2-amine | HCID 57762548 | — |
| Product | HCID 57762546 | HCID 57762546 | 94.9% |
Reaction Steps
In the same manner as in Reference Example 13, N-(4-iodophenyl)pyrimidin-2-amine (150 mg) and 1-bromo-3-methyl-2-butene (90 mg) were reacted in the presence of sodium hydride to obtain N-(4-iodophenyl)-N-(3-methyl-2-butenyl)pyrimidin-2-amine (175 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09162988B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-ee290c55e5d444778d7e46a602641093 |
| Source note | uspto-grants-2015_10 |