Hydrochloric Acid → HCID 67773047, compound

Participants

Reaction Steps

N,N-dimethyl-N′-(2-n-propylamino-7-methyl-pyrrolo[2,3 d]pyrimidin-4-yl)-hydrazine (100 mg, 0.4 mmol) was dissolved in H2O (5 mL) and 0.5 M aqueous HCl solution (1 mL) and the solution was lyophilized to yield N,N-dimethyl-N′-(2-n-propylamino-7-methyl-pyrrolo[2,3-d]pyrimidin-4-yl)-hydrazine hydrochloride (110 mg) as a yellow oil. LCMS (ESI) m/z=249 (M+H)+. 1H NMR (500 MHz, MeOD) δ (ppm) 6.92 (d, J=4.0 Hz, 1H), 6.50 (d, J=3.0 Hz, 1H), 3.66 (s, 3H), 3.45 (t, J=7.5 Hz, 2H), 2.79 (s, 6H), 1.67-1.72 (m, 2H), 1.01-1.04 (m, 3H).

Provenance & Evidence