HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexane → 2-[4-(Phenanthren-9-yl)phenyl]dibenzo[f,h]quinoxaline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexane | HCID 8058 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | 2-Chlorodibenzo[f,h]quinoxaline | HCID 58019496 | — |
| Product | 2-[4-(Phenanthren-9-yl)phenyl]dibenzo[f,h]quinoxaline | HCID 86679313 | — |
Reaction Steps
The Rf values of the objective substance and 2-chlorodibenzo[f,h]quinoxaline were respectively 0.20 and 0.55, which were found by silica gel thin layer chromatography (TLC) (with a developing solvent of ethyl acetate and hexane in a ratio of 1:10).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09162990B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-6cfc9729740b436383b214f5225adbed |
| Source note | uspto-grants-2015_10 |