HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 15886922, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | 3-Methoxy-9H-carbazole | HCID 519621 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 15886922 | HCID 15886922 | — |
Reaction Steps
3-Methoxy-9H-carbazole (Bedford, R. B.; Betham, M. J. Org. Chem. 2006, 71, 9403-9410) (0.029 g, 0.147 mmol) was dissolved in dry DMF (0.28 mL) and NBS (0.026 g, 0.147 mmol) was added to the solution. The reaction mixture was stirred at room temperature for 2 h under absence of light. The solution was poured into water (2 mL), filtered and washed with water. The title compound was isolated as a grey solid (0.033 g, 82%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09162980B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-3d69566c8d5c4395bfedff80b408cec2 |
| Source note | uspto-grants-2015_10 |