HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 24274903, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1-(2-Bromoethyl)-4-methoxybenzene | HCID 84427 | — |
| Reactant | N-Benzylidene(piperidin-4-yl)methanamine | HCID 11820173 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 24274903 | HCID 24274903 | — |
Reaction Steps
To a stirred solution of N-[phenylmethylidene]-1-(piperidin-4-yl)methanamine (compound iii; 0.158 moles; 31.9 g), prepared as described in WO2004/101548 in absolute ethanol (70 ml), 1-(2-bromoethyl)-4-methoxybenzene (compound iv; 0.237 moles; 32.7 g) and potassium carbonate were added.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09163013B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-7068fb79f45449d1a3ba540040acc96a |
| Source note | uspto-grants-2015_10 |