HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(4-Fluorophenoxy)ethanol → 5,7-Diethyl-2-[2-(4-fluorophenoxy)ethoxy]-[1,2,4]triazolo[1,5-a]pyrimidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(4-Fluorophenoxy)ethanol | HCID 574361 | — |
| Reactant | 2-Methanesulfonyl-5,7-diethyl-[1,2,4]triazolo[1,5-a]pyrimidine | HCID 86719320 | — |
| Product | 5,7-Diethyl-2-[2-(4-fluorophenoxy)ethoxy]-[1,2,4]triazolo[1,5-a]pyrimidine | HCID 76684795 | 70% |
Reaction Steps
The title compound was prepared according to the experimentals described for Example 14 above from 2-methanesulfonyl-5,7-diethyl-[1,2,4]triazolo[1,5-a]pyrimidine and 2-(4-fluorophenoxy)ethan-1-ol in 70% yield. EM (calc.): 330.1; MS (ESI) m/e: 331.3 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09163027B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-cc15693e6734439bb45be2e289715253 |
| Source note | uspto-grants-2015_10 |