HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Phenyl diethanolamine → 2-{[2-({5,7-Diethyl-[1,2,4]triazolo[1,5-a]pyrimidin-2-yl}oxy)ethyl](phenyl)amino}ethan-1-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Phenyl diethanolamine | HCID 8416 | — |
| Reactant | 2-Methanesulfonyl-5,7-diethyl-[1,2,4]triazolo[1,5-a]pyrimidine | HCID 86719320 | — |
| Product | 2-{[2-({5,7-Diethyl-[1,2,4]triazolo[1,5-a]pyrimidin-2-yl}oxy)ethyl](phenyl)amino}ethan-1-ol | HCID 76684790 | 43% |
Reaction Steps
The title compound was prepared according to the experimentals described for Example 14 above from 2-methanesulfonyl-5,7-diethyl-[1,2,4]-triazolo[1,5-a]pyrimidine and N-phenyldiethanolamine in 43% yield. EM (calc.): 355.2; MS (ESI) m/e: 356.3 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09163027B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-ccc572f1ac0d472384f3381a855365a1 |
| Source note | uspto-grants-2015_10 |