HuagongsheHuagongshe Chemistry Print Report · For research reference only
(5-Chloropyridin-2-yl)acetic acid → HCID 118341235, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (5-Chloropyridin-2-yl)acetic acid | HCID 46737473 | — |
| Reactant | HCID 90093760 | HCID 90093760 | — |
| Product | HCID 118341235 | HCID 118341235 | — |
Reaction Steps
Prepared according to Method M (Example 206) using (5-chloropyridin-2-yl)acetic acid (Preparation 80) and (5-aminopyridin-3-yl)[7-fluoro-1-(2-hydroxy-1-methylethyl)-1H-pyrrolo[3,2-c]pyridin-3-yl]methanone (Enantiomer 2, Preparation 26). The residue was purified using preparative TLC eluting with 5% MeOH in EtOAc.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09163021B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-16644342c7574a4fbb2412dad0d4a3b7 |
| Source note | uspto-grants-2015_10 |