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HRID1753052

反应详情

EQUATION

反应方程式

HRID 1753052 的结构方程式

REACTANTS

反应物

2
结构：CON(C)C(=O)c1cc(Br)ccn1
HCID58191769

未命名化合物

结构：CC(CO[Si](C)(C)C(C)(C)C)n1cc(I)c2cnccc21
HCID90093728

未命名化合物

PRODUCTS

生成物

1
结构：CC(CO[Si](C)(C)C(C)(C)C)n1cc(C(=O)c2cc(Br)ccn2)c2cnccc21
HCID90094032

未命名化合物

PROCEDURE

实验过程

Prepared according to the method described for Preparation 37 using 1-(2-{[tert-butyl(dimethyl)silyl]oxy}-1-methylethyl)-3-iodo-1H-pyrrolo[3,2-c]pyridine (Preparation 55) and 4-bromo-N-methoxy-N-methylpyridine-2-carboxamide. Purified using silica gel column chromatography eluting with 35-40% EtOAc in hexane.

WORKUP

后处理

  1. customPrepared
  2. customPurified
  3. washeluting with 35-40% EtOAc in hexane