HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-N-methoxy-N-methylpicolinamide → HCID 90094032, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-N-methoxy-N-methylpicolinamide | HCID 58191769 | — |
| Reactant | HCID 90093728 | HCID 90093728 | — |
| Product | HCID 90094032 | HCID 90094032 | — |
Reaction Steps
Prepared according to the method described for Preparation 37 using 1-(2-{[tert-butyl(dimethyl)silyl]oxy}-1-methylethyl)-3-iodo-1H-pyrrolo[3,2-c]pyridine (Preparation 55) and 4-bromo-N-methoxy-N-methylpyridine-2-carboxamide. Purified using silica gel column chromatography eluting with 35-40% EtOAc in hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09163021B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-0b997b6cf42344a68a60825571e39b94 |
| Source note | uspto-grants-2015_10 |