HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methyl-3-pentanone → 1-(Dimethylamino)-2,4-dimethylpent-1-en-3-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methyl-3-pentanone | HCID 11265 | — |
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Product | 1-(Dimethylamino)-2,4-dimethylpent-1-en-3-one | HCID 77230315 | — |
Reaction Steps
2-Methyl-3-pentanone (5 g, 49.9 mmol) and DMF-DMA (10 mL, 74.9 mmol) were heated together in a sealed tube for 4 days. The reaction was concentrated in vacuo to afford an orange oil that was used directly in the next reaction (1.64 g, 21%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09163021B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-48abf196fa1645838d9ff75f016dce50 |
| Source note | uspto-grants-2015_10 |