反应详情

2-Methyl-3-pentanone (5 g, 49.9 mmol) and DMF-DMA (10 mL, 74.9 mmol) were heated together in a sealed tube for 4 days. The reaction was concentrated in vacuo to afford an orange oil that was used directly in the next reaction (1.64 g, 21%).

1. concentrationThe reaction was concentrated in vacuo
2. customto afford an orange oil that
3. customwas used directly in the next reaction (1.64 g, 21%)