Cyclohexane → Cyclohexane ethylacetate

HRID 1753260Notes

Reaction equation

HRID 1753260 reaction equation
[CH2:1]1[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[C:7]([O:10][CH2:11][CH3:12])(=[O:9])[CH3:8]>>[CH2:1]1[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[C:7]([O:10][CH2:11][CH3:12])(=[O:9])[CH3:8]

Participants

3

Reactant 2

HCID 8078CyclohexaneHCID 8857Ethyl Acetate

Product 1

HCID 21867204Cyclohexane ethylacetate

Procedure

Method 1 was employed to produce MA/MVE polymer branched by DVI from a blend of cyclohexane and ethyl acetate (in equal mass ratio). For this synthesis, 47 g of MVE, 40 g of MA, 0.22 g of DVI, and 0.32 g of DCP were used to create of polymer having 50 mol % MVE, 49.82 mol % MA, and 0.18 mol % (or 3,500 ppm) DVI.

Workup

  1. customto produce MA/MVE polymer
  2. customFor this synthesis, 47 g of MVE, 40 g of MA, 0.22 g of DVI, and 0.32 g of DCP

Sources & evidence

ORD record
ord-89f345c217bd4546920369944c66d00d
Source dataset
uspto-grants-2015_10
Patent number
US09163102B2

Reaction notes

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