Hydrochloric Acid → HCID 67979862, compound

Participants

Reaction Steps

A mixture of 5 (4.2 g, 6.1 mmol) and NaOH (0.49 g, 12.2 mmol) in EtOH (80 mL) was refluxed for 6 h. The mixture was poured into water (400 mL). The pH was adjusted to 1 with aqueous 10 M HCl solution. The precipitated solid was collected by filtration and dried under vacuum. The crude product was used for the next step without any purification (3.9 g, 98% yield).

Provenance & Evidence