huagongshe.com
HRID1753834

反应详情

EQUATION

反应方程式

HRID 1753834 的结构方程式

REACTANTS

反应物

2
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：CC(C)(C)COc1ccc(-n2[nH]cc(-n3ccnn3)c2=O)nc1
HCID59603553

2-[5-(2,2-Dimethylpropoxy)-2-pyridinyl]-1,2-dihydro-4-(1H-1,2,3-triazol-1-yl)-3H-pyrazol-3-one

C15H18N6O2

PRODUCTS

生成物

1
结构：CC(C)(C)COc1ccc(-n2[nH]cc(-n3ccnn3)c2=O)nc1.Cl
HCID67457737

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1COCCO1
溶剂HCID31275

1,4-Dioxane

C4H8O2

PROCEDURE

实验过程

2 ml of a 4 N solution of hydrogen chloride in dioxane are added to 22 mg (0.1 mmol) of the compound from Example 84 and the mixture is stirred at RT for 1 h. The solid is filtered off and dried under a high vacuum.

WORKUP

后处理

  1. filtrationThe solid is filtered off
  2. customdried under a high vacuum