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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1753841Generated: October 28, 2026

Hydrochloric Acid → HCID 67457458, compound

https://huagongshe.com/reaction/1753841

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 86648148HCID 86648148—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 67457458HCID 67457458—

Reaction Steps

2.5 ml of a 4 N solution of hydrogen chloride in dioxane are added to 80 mg (0.2 mmol) of the compound from Example 94 and the mixture is stirred at RT for 1 h. The solid is filtered off, washed in each case once with dioxane and tert-butyl methyl ether and subsequently dried under a high vacuum.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09168249B2
Source datasetuspto-grants-2015_10
ORD IDord-0348170f75554c0a8ae4f655fb4cd426
Source noteuspto-grants-2015_10