HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 89454054, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 86730104 | HCID 86730104 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 89454054 | HCID 89454054 | 75% |
Reaction Steps
The product is obtained according to the procedure described in Step 1.7. by treating 8-fluoro-7-(pyrid-2-yl)-2-(tetrahydro-2H-pyran-2-yl)-5-(2,2,2-trifluoroethyl)-1,5-dihydro-4H-pyrazolo[4,3-c]quinolin-4-one with HCl in dioxane (4M). It is in the form of a white powder (hydrochloride; yield 75%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09169246B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-adc6b75b5e3044aeac8d17bc7e2cae47 |
| Source note | uspto-grants-2015_10 |