4-Nitrobenzyl chloride → HCID 71677842, compound

Participants

Reaction Steps

A solution of 1.716 g (10 mmol) 4-nitrobenzyl chloride and 1.152 g (10 mmol) tetrahydro-[1,3]oxazolo[2,3-b][1,3]oxazole in 20 ml of chloroform was stirred at the room temperature for 3 days. The precipitate was filtered off, washed twice with dichloromethane and dried. 2.161 g (75.4%) of white amorphous product was obtained, which can be further purified by recrystallisation from rectified ethanol.

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