alpha-Chloro-m-nitrotoluene → HCID 71677844, compound

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Reaction Steps

A solution of 1.716 g (10 mmol) 3-nitrobenzyl chloride and 1.152 g (10 mmol) tetrahydro-[1,3]oxazolo[2,3-b][1,3]oxazole in 20 ml of chloroform was stirred at the room temperature for 3 days. The precipitate was filtered off, washed twice with dichloromethane and dried. 1.894 g (66.1%) of white amorphous product was obtained, which can be further purified by recrystallisation from rectified ethanol.

Provenance & Evidence