2-Hydroxyethyl Methacrylate → Dmapma hema

HRID 1755199ノート

反応式

HRID 1755199 の反応式
[CH:1]([CH:3]1[CH2:10][CH2:9][CH2:8][CH2:7][NH:6][C:4]1=[O:5])=C.[CH3:11][N:12](CCCC=C(C)C(N)=O)[CH3:13].[C:23]([O:28][CH2:29][CH2:30][OH:31])(=[O:27])[C:24]([CH3:26])=[CH2:25]>O>[CH3:1][C:3]([C:4]([NH:6][CH2:7][CH2:8][CH2:9][N:12]([CH3:13])[CH3:11])=[O:5])=[CH2:10].[CH3:26][C:24]([C:23]([O:28][CH2:29][CH2:30][OH:31])=[O:27])=[CH2:25]

参加物

5

反応物 3

HCID 133602-Hydroxyethyl MethacrylateHCID 17881685Vinyl caprolactamHCID 20976834Dimethylaminopropylmethacrylamide

生成物 1

HCID 87665647Dmapma hema

試薬・触媒・溶媒 1

HCID 962Water溶媒

反応条件

温度
60 °C

実験手順

Five hundred grams (500 g) of de-ionized water was added to 1000 g of a 30% aqueous solution of a terpolymer of vinyl caprolactam (VCap), dimethylamino propyl methacrylamide (DMAPMA), and 2-hydroxyethyl methacrylate (HEMA). GMA (12 g) was added drop-wise with continuous stirring. The obtained solution was heated at 60° C. for one hour. The resulting product was freeze dried to render a solid, white powder. A representative structure for the polymeric reaction is presented below, wherein x+y+z+a=100:

後処理

  1. additionGMA (12 g) was added drop-wise with continuous stirring
  2. customdried
  3. customA representative structure for the polymeric reaction

出典と根拠

ORDレコード
ord-379a6f9b7afb43deb4ee664df1106e02
出典データセット
uspto-grants-2015_10
特許番号
US09169344B2

反応ノート

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