反应详情

温度

80 °C

Following the general procedure as described in Example 117, except using material from Example 106 (100 mg, 0.259 mmol), 1,2-dichloroethane (2.5 mL), trimethylstannanol (140 mg, 0.0.776 mmol), and heating in a microwave for 2.5 h at 80° C. under normal power, 41.4 mg (43%) of the title compound is isolated as a thick oil that contains 0.25 equivalents of the tin reagent. LC/MS (Condition A): ret. T=2.28 min, (M+H)+ 373.