HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 86748822, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | N-[(6-Chloro-3-pyridinyl)methyl]-N,N′-dimethyl-2-nitro-1,1-ethenediamine | HCID 85054604 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 86748822 | HCID 86748822 | 102.8% |
Reaction Steps
A mixture of 1-[N-(6-chloro-3-pyridylmethyl)-N-methylamino]-1-methylamino-2-nitroethylene(0.39 g), 37% aqueous solution of formaldehyde (0.16 g), 50% aqueous solution of dimethylamine (0.18 g) and acetonitrile (3 ml) was stirred at room temperature for 8.5 hours. The reaction mixture was concentrated to give 1-[N-(6-chloro-3-pyridylmethyl)-N-methylamino]-3-dimethylamino-1-methylamino-2-nitro-propene (Compound No. 1) (0.49 g) as a syrupy liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05438065 |
| Source dataset | uspto-grants-1995_08 |
| ORD ID | ord-033e682bc3a04948a875b46231afa2e8 |
| Source note | uspto-grants-1995_08 |