HCID 22406184, compound → HCID 23720264, compound

HRID 1755771Notes

Reaction equation

HRID 1755771 reaction equation
[CH:1]1[CH:6]=[C:5]([OH:7])[C:4]([S:8]([O-:11])(=[O:10])=[O:9])=[CH:3][CH:2]=1.[Na+:12].[C:13]1(=[O:29])[N:17]([CH:18]([CH3:23])[CH2:19][C:20](Cl)=[O:21])[C:16](=[O:24])[C:15]2=[CH:25][CH:26]=[CH:27][CH:28]=[C:14]12>C1(C)C(C)=CC=CC=1>[C:16]1(=[O:24])[N:17]([CH:18]([CH3:23])[CH2:19][C:20]([O:7][C:5]2[CH:6]=[CH:1][CH:2]=[CH:3][C:4]=2[S:8]([O-:11])(=[O:9])=[O:10])=[O:21])[C:13](=[O:29])[C:14]2=[CH:28][CH:27]=[CH:26][CH:25]=[C:15]12.[Na+:12]

Participants

4

Reactant 2

HCID 22406184HCID 22406184, compoundHCID 23674503Sodium o-phenolsulfonate

Product 1

HCID 23720264HCID 23720264, compound

Reagents, catalysts & solvents 1

HCID 7237O-XyleneSolvent

Procedure

148.0 g (755 mmol) of anhydrous sodium phenolsulfonate and 190.0 g (755 mmol) of γ-phthalimidobutanoyl chloride are reacted in 200 g of xylene at 140° C. for 4 hours and the mixture is worked up as in Example 1. The crude product is recrystallized from methanol and the white crystalline product is dried at 40° C. under a water pump vacuum.

Workup

  1. customThe crude product is recrystallized from methanol
  2. customthe white crystalline product is dried at 40° C. under a water pump vacuum

Sources & evidence

ORD record
ord-d40e45448f6a4ccb876a3b998faf4d49
Source dataset
uspto-grants-1995_08
Patent number
US05438147

Reaction notes

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