HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 70083987, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 70085396 | HCID 70085396 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 70083987 | HCID 70083987 | — |
Reaction Steps
To a stirred solution of 30 mg of (40) in CH2Cl2 (1 mL) was added trifluoroacetic acid (10 mL). After stirring for 45 min the reaction was evaporated to dryness, triturated with ether, filtered and dried under vacuum to give the title compound (41) as a mixture of isomers (24rag, 75%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05438118 |
| Source dataset | uspto-grants-1995_08 |
| ORD ID | ord-713cc8ccd8a742bd8658c5000fda9341 |
| Source note | uspto-grants-1995_08 |