HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → HCID 11075340, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | 2,2-Dimethyl-1,3-dioxane-4,6-dione | HCID 16249 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 11075340 | HCID 11075340 | — |
Reaction Steps
Meldrum's acid (73) is treated with benzaldehyde in the presence of borane-triethylamine complex in toluene. The product is isolated by flash chromatography over silica gel to give (74).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05438118 |
| Source dataset | uspto-grants-1995_08 |
| ORD ID | ord-86569f27a1064d99964ab736ddfa01c7 |
| Source note | uspto-grants-1995_08 |