HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenethyl bromide → HCID 67780719, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenethyl bromide | HCID 7666 | — |
| Reactant | 2-Methyl-7-azaindole | HCID 583066 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 67780719 | HCID 67780719 | 92.6% |
Reaction Steps
A solution of 85 mg (0.64 mmol) of 2-methyl-pyrrolo[2,3-b]pyridine and 140 mg(0.76 mmol) of (2-bromoethyl)benzene in 1 ml acetonitrile was refluxed for 40 h. The solvent was evaporated and the residue was treated with ether. The solid that formed was isolated by filtration to give 188 mg (62%) of 2-methyl-7- (2-phenylethyl)pyrrolo[2,3-b]pyridinehydrobromide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05439917 |
| Source dataset | uspto-grants-1995_08 |
| ORD ID | ord-f4a8dc231ed4479ab1db8ae1c538cb6f |
| Source note | uspto-grants-1995_08 |