HRID1756045

反应详情

EQUATION

反应方程式

HRID 1756045 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A solution of 0.3 g (2.3 mmol) 3-methylpyrrolo[2,3-b]pyridine and 0.5 g (2.7 mmol) (2-bromoethyl)benzene in 10 ml acetonitril was refluxed for 72 h. The solvent was evaporated and the solid that formed was treated with ether. Recrystalization from ethyl acetate gave 0.2 g (27%) of the title compound as a white solid.

WORKUP

后处理

  1. customThe solvent was evaporated
  2. customthe solid that formed
  3. customRecrystalization from ethyl acetate