HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenethyl bromide → HCID 19916790, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenethyl bromide | HCID 7666 | — |
| Reactant | 3-Methyl-1H-pyrrolo[2,3-b]pyridine-2-methanol | HCID 19392613 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 19916790 | HCID 19916790 | — |
Reaction Steps
A solution of 0.11 g (0.68 mmol) 2-hydroxymethyl-3-methylpyrrolo [2,3-b]pyridine and 0.13 g (7 mmol) (2-bromoethyl)benzene in 5 ml acetonitril was refluxed for 24 h. The solvent was evaporated. Chromatography on silica gel eluting with methylene chloride and methanol (10:1) gave the desired product. (0.03 g 13%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05439917 |
| Source dataset | uspto-grants-1995_08 |
| ORD ID | ord-4c2b772875214f91a2ac770bd11c61d2 |
| Source note | uspto-grants-1995_08 |