2-Chloroacetophenone → HCID 19916806, compound

Participants

Reaction Steps

2-Methyl-pyrrolo[2,3-b]pyridine (0.5 g, 3.78 mmol), phenacyl chloride (0.62 g, 4.0 mmol ) and acetonitrile (10 ml) were refluxed for 12 h. The solid was filtered off and washed with cold carbon tetrachlorid (2 ml). The crude product was recrystallized from chloroform/ether, 1:1, to give 0.95 g (88%) title compound.

Provenance & Evidence