HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloroacetophenone → HCID 131719075, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloroacetophenone | HCID 10757 | — |
| Reactant | 3-Methoxy-2-methyl-1H-pyrrolo[2,3-b]pyridine | HCID 19916818 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 131719075 | HCID 131719075 | 34.3% |
Reaction Steps
A solution of 0,75 g (4,6 mmol) 3-methoxy-2-methylpyrrolo[2,3-b]pyridine and 0,75 g (4,8 mmol) phenacyl chloride in 50 ml acetonitrile was refluxed for 14 h. Working up in the same manner as ex. 17 gave 0,5 g (34%) of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05439917 |
| Source dataset | uspto-grants-1995_08 |
| ORD ID | ord-093bd02bf22346cca72c635684b1322f |
| Source note | uspto-grants-1995_08 |