HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3-Dimethyl-1H-pyrrolo[2,3-b]pyridine → 2,3-Dimethyl-7-(o-methylthiophenacyl)pyrrolo[2,3-b]pyridinehydrobromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3-Dimethyl-1H-pyrrolo[2,3-b]pyridine | HCID 12532387 | — |
| Reactant | o-Methylthiophenacyl bromide | HCID 54146844 | — |
| Product | 2,3-Dimethyl-7-(o-methylthiophenacyl)pyrrolo[2,3-b]pyridinehydrobromide | HCID 19392594 | 20.9% |
Reaction Steps
A solution of 0,2 g (1,4 mmol) 2,3-dimethylpyrrolo[2,3-b]pyridine and 0,34 g (1,4 mmol) o-methylthiophenacyl bromide was stirred at room temperature for 4 h. The precipitated product was filtred off and dried affording 0,11 g (20%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05439917 |
| Source dataset | uspto-grants-1995_08 |
| ORD ID | ord-48e92292ffad4566b875e2bc85125334 |
| Source note | uspto-grants-1995_08 |