HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 19916763, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | 2-Bromo-4'-methylacetophenone | HCID 69272 | — |
| Reactant | 2,3-Dimethyl-1H-pyrrolo[2,3-b]pyridine | HCID 12532387 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 19916763 | HCID 19916763 | — |
Reaction Steps
A solution of 2,3-dimethylpyrrolo[2,3-b]pyridine (0.16 g, 1.1 mmol) and p-methylphenacyl bromide (0.26 g, 1.2 mmol) in 4.5 ml CH3CN was warmed to reflux which was enough to initiate crystallisation of the product as a light yellow solid. The precipitate was isolated as described in example 27 furnishing 0.29 g (74%) pure hydrobromide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05439917 |
| Source dataset | uspto-grants-1995_08 |
| ORD ID | ord-45fa9973ee864dd5bd374d579276aa1b |
| Source note | uspto-grants-1995_08 |