HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetonitrile → HCID 19392596, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | 2-Chloroacetophenone | HCID 10757 | — |
| Reactant | HCID 70347403 | HCID 70347403 | — |
| Product | HCID 19392596 | HCID 19392596 | 58% |
Reaction Steps
A solution of 1.0 g (5.8 mmol) of 3-cyano-methyl-2-methyl pyrrolo[2,3-b]pyridine and 1.08 g (7.0 mmol) of phenacyl chloride in 50 ml acetonitrile was refluxed for 14 h. Working up in the same manner as described in example 17 gave 0,5 g 58% of the desired title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05439917 |
| Source dataset | uspto-grants-1995_08 |
| ORD ID | ord-1aeb9be6dee842fb9a9f4d7a338a8903 |
| Source note | uspto-grants-1995_08 |