HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenacyl bromide → HCID 19916770, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenacyl bromide | HCID 6259 | — |
| Reactant | HCID 22477320 | HCID 22477320 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 19916770 | HCID 19916770 | 70.9% |
Reaction Steps
3-(Cyanomethyl)-2-phenylpyrrolo[2,3-b]pyridine (0.35 g, 1.5 mmol) and phenacyl bromide (0.36 g) in acetonitrile (5 ml) was refluxed for 18 h. The resulting solid product was isolated by filtration and washed with diethyl ether to give pure 3-(cyanomethyl)-7-phenacyl-2-phenylpyrrolo[2,3-b]pyridine hydrobromide (0.46 g, 70%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05439917 |
| Source dataset | uspto-grants-1995_08 |
| ORD ID | ord-ff78333b318c49ecbeb12698bcda7ca3 |
| Source note | uspto-grants-1995_08 |