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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1756089Generated: October 27, 2026

Phenacyl bromide → HCID 19916770, compound

https://huagongshe.com/reaction/1756089

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPhenacyl bromideHCID 6259—
ReactantHCID 22477320HCID 22477320—
SolventAcetonitrileHCID 6342—
ProductHCID 19916770HCID 1991677070.9%

Reaction Steps

3-(Cyanomethyl)-2-phenylpyrrolo[2,3-b]pyridine (0.35 g, 1.5 mmol) and phenacyl bromide (0.36 g) in acetonitrile (5 ml) was refluxed for 18 h. The resulting solid product was isolated by filtration and washed with diethyl ether to give pure 3-(cyanomethyl)-7-phenacyl-2-phenylpyrrolo[2,3-b]pyridine hydrobromide (0.46 g, 70%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05439917
Source datasetuspto-grants-1995_08
ORD IDord-ff78333b318c49ecbeb12698bcda7ca3
Source noteuspto-grants-1995_08