Hydrochloric Acid → HCID 14822310, compound
Reaction equation
Cl.[CH2:2]([N:9]1[C:13]([CH2:14][CH2:15][CH:16]=[C:17]([C:24]2[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=2)[C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)=[CH:12][N:11]=[CH:10]1)[C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.Cl>C(O)C>[CH2:2]([N:9]1[C:13]([CH2:14][CH2:15][CH2:16][CH:17]([C:24]2[CH:25]=[CH:26][CH:27]=[CH:28][CH:29]=2)[C:18]2[CH:19]=[CH:20][CH:21]=[CH:22][CH:23]=2)=[CH:12][N:11]=[CH:10]1)[C:3]1[CH:4]=[CH:5][CH:6]=[CH:7][CH:8]=1Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
1-benzyl-5-(4,4-diphenyl-3-butenyl)-1H-imidazole hydrochloride salt is hydrogenated in ethanol as described in Example 1 c). M.p. of the product as hydrochloride is 200°-202° C.
Workup
- customis 200°-202° C.
Sources & evidence
- ORD record
- ord-cee6d769005f47a2b056518ae26002ce
- Source dataset
- uspto-grants-1995_08
- Patent number
- US05439928
Reaction notes
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