Benzyl Bromide → HCID 21474551, compound

HRID 1756442Notes

Reaction equation

HRID 1756442 reaction equation
[C:1]([O:5][C:6]([CH2:8][C:9]1[CH:17]=[CH:16][C:12]([C:13]([OH:15])=[O:14])=[CH:11][CH:10]=1)=[O:7])([CH3:4])([CH3:3])[CH3:2].[CH2:18](Br)[C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1>>[CH2:18]([O:14][C:13]([C:12]1[CH:11]=[CH:10][C:9]([CH2:8][C:6]([O:5][C:1]([CH3:4])([CH3:2])[CH3:3])=[O:7])=[CH:17][CH:16]=1)=[O:15])[C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1

Participants

3

Reactant 2

HCID 7498Benzyl BromideHCID 21474481HCID 21474481, compound

Product 1

HCID 21474551HCID 21474551, compound

Procedure

In a manner similar to Example 7(a), by reaction of 3 g (12.7 mmol) of 4-(tert-butoxycarbonylmethyl)benzoic acid prepared in Example 29(a) with 1.6 ml (14 mmol) of benzyl bromide, 3.2 g (77%) of the benzyl ester are obtained in the form of a slightly yellow oil.

Workup

  1. customare obtained in the form of a slightly yellow oil

Sources & evidence

ORD record
ord-1e7d273ff77e422b9e26c54212988349
Source dataset
uspto-grants-1995_08
Patent number
US05439925

Reaction notes

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